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Biblioteca (s) : |
INIA Las Brujas. |
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Fecha : |
10/07/2019 |
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Actualizado : |
10/07/2019 |
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Tipo de producción científica : |
Artículos en Revistas Indexadas Internacionales |
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Autor : |
BESIL, N.; REZENDE, S.; ALONZO, N.; CESIO, M.V.; RIVAS, F.; HEINZEN, H. |
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Afiliación : |
NATALIA BESIL, Grupo de Análisis de Compuestos Traza (GACT), Departamento de Química del Litoral, Facultad de Química, CENUR Litoral Norte, Universidad de la República.; SOFÍA REZENDE, Grupo de Análisis de Compuestos Traza (GACT), Departamento de Química del Litoral, Facultad de Química, CENUR Litoral Norte, Universidad de la República, Paysandú, Uruguay.; NOEL ALONZO, Grupo de Análisis de Compuestos Traza (GACT), Departamento de Química del Litoral, Facultad de Química, CENUR Litoral Norte, Universidad de la República, Paysandú, Uruguay.; MARÍA VERÓNICA CESIO, Grupo de Análisis de Compuestos Traza (GACT), Departamento de Química del Litoral, Facultad de Química, CENUR Litoral Norte, Universidad de la República, Paysandú, Uruguay.; CARLOS FERNANDO RIVAS GRELA, INIA (Instituto Nacional de Investigación Agropecuaria), Uruguay; HORACIO HEINZEN, Grupo de Análisis de Compuestos Traza (GACT), Departamento de Química del Litoral, Facultad de Química, CENUR Litoral Norte, Universidad de la República, Paysandú, Uruguay. |
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Título : |
Analytical methods for the routinely evaluation of pesticide residues in lemon fruits and by products. |
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Complemento del título : |
Research article. |
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Fecha de publicación : |
2019 |
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Fuente / Imprenta : |
SN Applied Sciences, 2019, 1: 618. |
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ISSN : |
2523-3971 |
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DOI : |
10.1007%2Fs42452-019-0626-x |
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Idioma : |
Inglés |
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Notas : |
Article history: Received: 10 October 2018 / Accepted: 16 May 2019 / Published online: 22 May 2019. |
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Contenido : |
ABSTRACT.
Citrus fruits and their by-products such as concentrated juices and essential oils are important intermediate by-products in the food industry that can selectively accumulate plant protection agrochemicals employed in their production. They are very difcult matrices for pesticide residue analysis due their high number and concentration of phytochemicals that could hamper the determinations. The fruit processing leads to the concentration/dilution or elimination of some of these natural products that change totally the nature of the matrix where the pesticides partition unevenly. Looking at the industrial process of the fruit, a unifed vision for the pesticide residues analysis throughout the lemon fruit chain production, useful for the routine analysis of the above mentioned three matrices is presented. The driven concept is the minimization of matrix efects through sample dilution of the concentrated by-products, either after sample treatment or not. This approach will contribute to the maintenance of the whole instrumental system. QuEChERS AOAC 2007.01 was selected as the most suitable protocol for routine determination of, residues of 16 the pesticides most commonly used in the fruits during the citrus production through liquid chromatography coupled to tandem mass spectrometry (LC?MS/MS). The same protocol was applied for pesticide residue analysis in concentrated juice after diluting 4 times the sample to minimize the matrix efects. For the analysis of lemon essential oils, the dilution and shoot procedure proved to be useful for LC?MS/MS and gas chromatography?mass spectrometry determination. The three methodologies were validated following SANTE guidelines, with quantitation limits below the established European Union and Codex Alimentarius maximum residue limits. The developed methodologies are useful tools for the routine control analysis of pesticide residues in lemon matrices, allowing high sample throughput and enhancing labs productivity.
© Springer Nature Switzerland AG MenosABSTRACT.
Citrus fruits and their by-products such as concentrated juices and essential oils are important intermediate by-products in the food industry that can selectively accumulate plant protection agrochemicals employed in their production. They are very difcult matrices for pesticide residue analysis due their high number and concentration of phytochemicals that could hamper the determinations. The fruit processing leads to the concentration/dilution or elimination of some of these natural products that change totally the nature of the matrix where the pesticides partition unevenly. Looking at the industrial process of the fruit, a unifed vision for the pesticide residues analysis throughout the lemon fruit chain production, useful for the routine analysis of the above mentioned three matrices is presented. The driven concept is the minimization of matrix efects through sample dilution of the concentrated by-products, either after sample treatment or not. This approach will contribute to the maintenance of the whole instrumental system. QuEChERS AOAC 2007.01 was selected as the most suitable protocol for routine determination of, residues of 16 the pesticides most commonly used in the fruits during the citrus production through liquid chromatography coupled to tandem mass spectrometry (LC?MS/MS). The same protocol was applied for pesticide residue analysis in concentrated juice after diluting 4 times the sample to minimize the matrix efects. For the analysis of lemon e... Presentar Todo |
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Palabras claves : |
CONCENTRATED LEMON JUICE; ESSENTIAL OILS; GC–MS; LC–MS/MS; LEMON FRUIT; PESTICIDE RESIDUES. |
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Asunto categoría : |
F01 Cultivo |
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Marc : |
LEADER 02922naa a2200289 a 4500
001 1059939
005 2019-07-10
008 2019 bl uuuu u00u1 u #d
022 $a2523-3971
024 7 $a10.1007%2Fs42452-019-0626-x$2DOI
100 1 $aBESIL, N.
245 $aAnalytical methods for the routinely evaluation of pesticide residues in lemon fruits and by products.$h[electronic resource]
260 $c2019
500 $aArticle history: Received: 10 October 2018 / Accepted: 16 May 2019 / Published online: 22 May 2019.
520 $aABSTRACT. Citrus fruits and their by-products such as concentrated juices and essential oils are important intermediate by-products in the food industry that can selectively accumulate plant protection agrochemicals employed in their production. They are very difcult matrices for pesticide residue analysis due their high number and concentration of phytochemicals that could hamper the determinations. The fruit processing leads to the concentration/dilution or elimination of some of these natural products that change totally the nature of the matrix where the pesticides partition unevenly. Looking at the industrial process of the fruit, a unifed vision for the pesticide residues analysis throughout the lemon fruit chain production, useful for the routine analysis of the above mentioned three matrices is presented. The driven concept is the minimization of matrix efects through sample dilution of the concentrated by-products, either after sample treatment or not. This approach will contribute to the maintenance of the whole instrumental system. QuEChERS AOAC 2007.01 was selected as the most suitable protocol for routine determination of, residues of 16 the pesticides most commonly used in the fruits during the citrus production through liquid chromatography coupled to tandem mass spectrometry (LC?MS/MS). The same protocol was applied for pesticide residue analysis in concentrated juice after diluting 4 times the sample to minimize the matrix efects. For the analysis of lemon essential oils, the dilution and shoot procedure proved to be useful for LC?MS/MS and gas chromatography?mass spectrometry determination. The three methodologies were validated following SANTE guidelines, with quantitation limits below the established European Union and Codex Alimentarius maximum residue limits. The developed methodologies are useful tools for the routine control analysis of pesticide residues in lemon matrices, allowing high sample throughput and enhancing labs productivity. © Springer Nature Switzerland AG
653 $aCONCENTRATED LEMON JUICE
653 $aESSENTIAL OILS
653 $aGC–MS
653 $aLC–MS/MS
653 $aLEMON FRUIT
653 $aPESTICIDE RESIDUES
700 1 $aREZENDE, S.
700 1 $aALONZO, N.
700 1 $aCESIO, M.V.
700 1 $aRIVAS, F.
700 1 $aHEINZEN, H.
773 $tSN Applied Sciences, 2019, 1: 618.
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Registro original : |
INIA Las Brujas (LB) |
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Registro completo
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Biblioteca (s) : |
INIA Las Brujas; INIA Tacuarembó. |
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Fecha actual : |
21/02/2014 |
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Actualizado : |
21/02/2018 |
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Tipo de producción científica : |
Capítulo en Libro Técnico-Científico |
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Autor : |
NUÑEZ, S.; SCATONI, I.; CANESSA, S.; MUJICA, V.; PAULLIER, J. |
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Afiliación : |
SATURNINO NUÑEZ BUA, INIA (Instituto Nacional de Investigación Agropecuaria), Uruguay; IRIS SCATONI, Universidad de la República (UdelaR)/ Facultad de Agronomía; SANTIAGO CANESSA, Consultor Privado; MARÍA VALENTINA MUJICA TELIZ, Consultor Privado; JORGE ARTURO PAULLIER SUAREZ, INIA (Instituto Nacional de Investigación Agropecuaria), Uruguay. |
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Título : |
Plagas del duraznero: bioecologìa y daños. |
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Fecha de publicación : |
2010 |
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Fuente / Imprenta : |
ln: SORIA, J. (Ed). Manual del duraznero: manejo integrado de plagas y enfermedades. Montevideo (Uruguay): INIA, 2010. |
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Páginas : |
1-24 |
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Serie : |
(INIA Boletín de Divulgación; 99) |
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ISBN : |
978-9974-38-288-6 |
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ISSN : |
1510-7396 |
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Idioma : |
Español |
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Palabras claves : |
COCHINILLA BLANCA; COCHINILLA BLANCA DEL DURAZNERO; ESCAMA; GRAFOLITA; PIOJO DE SAN JOSE; TRIPS. |
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Thesagro : |
CONTROL DE PLAGAS; CYDIA MOLESTA; DAÑOS A LAS PLANTAS; DIADPIDIDAE; DURAZNO; ENEMIGOS NATURALES; METODOS DE CONTROL; PERIODICIDAD; PLAGAS; PRUNUS PERSICA; PSEUDAULACASPIS PENTAGONA; URUGUAY; VIGILANCIA. |
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Asunto categoría : |
--
H20 Enfermedades de las plantas |
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URL : |
http://www.ainfo.inia.uy/digital/bitstream/item/8740/1/Bd-99-p.1-24.pdf
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Marc : |
LEADER 01197naa a2200433 a 4500
001 1008869
005 2018-02-21
008 2010 bl uuuu u00u1 u #d
020 $a978-9974-38-288-6
022 $a1510-7396
100 1 $aNUÑEZ, S.
245 $aPlagas del duraznero$bbioecologìa y daños.
260 $c2010
300 $a1-24
490 $a(INIA Boletín de Divulgación; 99)
650 $aCONTROL DE PLAGAS
650 $aCYDIA MOLESTA
650 $aDAÑOS A LAS PLANTAS
650 $aDIADPIDIDAE
650 $aDURAZNO
650 $aENEMIGOS NATURALES
650 $aMETODOS DE CONTROL
650 $aPERIODICIDAD
650 $aPLAGAS
650 $aPRUNUS PERSICA
650 $aPSEUDAULACASPIS PENTAGONA
650 $aURUGUAY
650 $aVIGILANCIA
653 $aCOCHINILLA BLANCA
653 $aCOCHINILLA BLANCA DEL DURAZNERO
653 $aESCAMA
653 $aGRAFOLITA
653 $aPIOJO DE SAN JOSE
653 $aTRIPS
700 1 $aSCATONI, I.
700 1 $aCANESSA, S.
700 1 $aMUJICA, V.
700 1 $aPAULLIER, J.
773 $tln: SORIA, J. (Ed). Manual del duraznero: manejo integrado de plagas y enfermedades. Montevideo (Uruguay): INIA, 2010.
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